Quartz Deformation

We are conducting deformation experiments on Quartz using the D-DIA apparatus. The following is an example of the data we collect.

 

Portion of an x-ray diffraction pattern

Portion of an x-ray diffraction pattern showing the quartz (100)
peak in the compression and transverse detectors. The differential lattice strain (ehkl) is calculated from the difference in peak positions between the two sets of detectors.

 

 

Lattice spacings for the quartz (100) reflection.

Lattice spacing for the quartz (101) reflection.

Lattice spacing for the quartz (102) reflection.

Lattice spacings for the quartz (100), (101), and (112) reflections as a function of time during the deformation experiment. The calculated "hydrostatic" d-spacing is shown as a dashed line. The position of each reflection is measured as a function of time during the deformation experiment. D-spacings for the vertical pair of detectors (1 & 2) shrink more than for the horizontal pair (3 & 4), reflecting increasing differential stress.

 

 

We use Elastic-Plastic Self-Consistent (EPSC) Models to interpret our diffraction data. EPSC Models assume that ductile deformation is controlled by the motion of dislocations and/or by twinning.

Explanation of EPSC Model used

 

We were able to simulate our diffraction data collected at 800°C with an EPSC Model that used only basal and prismatic slip. This is consistent with the slip systems that are thought to operate at this temperature.

Parameters used in EPSC models

For out most recent poster on quartz deformation, click here.

Publications

Burnley, P.C. and Zhang, D. 2008 Interpreting in-situ x-ray diffraction data from high pressure deformation experiments using elastic plastic self consistent models: an example using quartz, Journal of Physics: Condensed Matter, v 20, doi:10.1088/0953-8984/20/28/285201, 10pp